Handbook of Chromatography
eBook - ePub

Handbook of Chromatography

Volume II: Polymers

  1. 238 pages
  2. English
  3. ePUB (mobile friendly)
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eBook - ePub

Handbook of Chromatography

Volume II: Polymers

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About This Book

Handbook of Chromatography features tables and chromatograms, theoretical discussions, and practical applications on the topic. Tables and chromatograms are based on polymer analyses abstracted from literature references dating from 1981-1991. Compounds presented in the tables and chromatograms include residual monomers, plasticizers, additives, antioxidants, and products from the thermal degradation (pyrolysis) of a broad range of synthetic polymers.
Theoretical discussions focus on new developments in the respective areas of gas, pyrolysis-gas, liquid, and size exclusion chromatographic separations. Capillary column technology, inverse gas chromatography (IGC), supercritical fluid extractions (SFE), and supercritical fluid chromatography (SFC) are also covered. A Practical Applications subsection provides a list of commercial suppliers of column packings and packed columns for gas and liquid chromatography. The book will be an excellent reference for chromatographers, organic chemists, and analytical chemists.

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Information

Publisher
CRC Press
Year
2020
ISBN
9781351089357
Edition
1
Topic
Physical Sciences
Subtopic
Chemistry
Index
Chemistry

Section IV

Chromatographic Tables and Figures

IV.1 GAS CHROMATOGRAPHY

Table GC1
ANALYSIS OF ACETALALDEHYDE RESIDUE IN PET (POLYETHYLENE TERPHTHALATE) BOTTLES
Sample preparation: The sample is ground in a liquid nitrogen mill and placed in a headspace vial. The vial is thermally equilibrated, and the contents of the headspace are automatically injected into the gas chromatograph.
Chromatographic conditions
Column
Material
Fused silica
Length, cm
2
Diameter, mm i.d.
1.8
Phase
Porapak Q
Temperature program
Isothermal at 135Ā°C
Compound
Retention time (min)
Acetaldehyde
2.0
Image
Dong, M. W., Chromatographia, 14(8), 447, 1981; reprinted with the permission of Vieweg & Sohn.
Table GC-2
VOLATILES RELEASED FROM POLY(VINYL CHLORIDE)
Sample preparation: Volatiles trapped on poly(phenylquinoxaline) absorbent.
Chromatographic conditions
Column
Material
Glass
Length, cm
2
Diameter, mm i.d.
2
Phase
3% OV-1 (80-100 mesh) on Gas Chrom Q
Carrier gas
He
Flow rate, cc/min
30
Temperature program
50Ā°C to 200Ā°C at ...

Table of contents

  1. Cover
  2. Series Page
  3. Title Page
  4. Copyright Page
  5. Series Preface
  6. Preface
  7. The Editor-in-Chief
  8. The Editors
  9. Table of Contents
  10. Section I: Principles and Techniques
  11. Section II: Practical Applications
  12. Section III: List of Tables and Figures
  13. Section IV: Tables and Chromatograms
  14. Section V: Compound Index