Laboratory Techniques in Electroanalytical Chemistry, Revised and Expanded

Peter Kissinger, Peter T. Kissinger, William R. Hieneman, William R. Heineman, Peter Kissinger, William R. Heineman

• Publisher: CRC Press
• Year: 2018
• ISBN:
  9781351990714
• Edition: 2
• Topic: Physical Sciences
• Subtopic: Analytic Chemistry

This volume provides a practical, intuitive approach to electroanalytical chemistry, presenting fundamental concepts and experimental techniques without the use of technical jargon or unnecessarily extensive mathematics. This edition offers new material on ways of preparing and using microelectrodes, the processes that govern the voltammetric behavior of microelectrodes, methods for characterizing chemically modified electrodes, electrochemical studies at reduced temperatures, and more. The authors cover such topics as analog instrumentation, overcoming solution resistance with stability and grace in potentiostatic circuits, conductivity and conductometry, electrochemical cells, carbon electrodes, film electrodes, microelectrodes, chemically modified electrodes, mercury electrodes, and solvents and supporting electrolytes.

Table of contents

• Cover
• Half Title
• Title Page
• Copyright Page
• Table of Contents
• Preface
• Contributors
• 1 An Overview
• 2 Fundamental Concepts of Analytical Electrochemistry
• 3 Large-Amplitude Controlled-Potential Techniques
• 4 Large-Amplitude Controlled-Current Techniques
• 5 Small-Amplitude Controlled-Potential Techniques
• 6 Introduction to Analog Instrumentation
• 7 Overcoming Solution Resistance with Stability and Grace in Potentiostatic Circuits
• 8 Conductivity and Conductometry
• 9 Electrochemical Cells
• 10 Carbon Electrodes
• 11 Film Electrodes
• 12 Microelectrodes
• 13 Chemically Modified Electrodes
• 14 Mercury Electrodes
• 15 Solvents and Supporting Electrolytes
• 16 Electrochemical Studies at Reduced Temperature
• 17 Electroanalytical Chemistry in Molten Salts
• 18 Vacuum-Line Techniques
• 19 Electrochemistry in the Dry Box
• 20 Digital Simulation of Electrochemical Problems
• 21 Evaluation of Mechanisms of Organic Reactions
• 22 Electroorganic Synthesis
• 23 Instructional Examples of Electrode Mechanisms of Transition Metal Complexes
• 24 Electrochemical Preconcentration
• 25 Controlled-Current Coulometry
• 26 Electrochemistry in Pharmaceutical Analysis
• 27 Electrochemical Detection in Liquid Chromatography and Capillary Electrophoresis
• 28 Photonic Electrochemistry
• 29 Principles and Techniques of Electrochemical-Electron Paramagnetic Resonance Experiments
• Index